Check the fittings on the tanks, hose and nozzle to ensure that they're tight. Put on safety goggles, gloves and a respirator.
Open the valves on the tanks that contain the chemicals for the insulation. Once they're mixed, they react to create the foam insulation.
Begin spraying the insulation onto one upper corner of the first wall. If needed, rent a hydraulic lift -- so you can access the higher sections of the wall. Move the gun back and forth, covering a section of the wall that measures 3 to 4 feet, and then moving onto the next section after the wall has been covered.
Spray the foam insulation onto every surface that needs to be insulated, then inspect the walls to see if you missed any spots. Apply more insulation if needed. The insulation only needs a few moments to cure.