Prepare the floor. If the existing is wood or concrete, rough the area with an orbital sander using 64-grit sandpaper. Remove any finish, such as varnish or paint. Sweep up any loose debris from the sanding with a broom.
Frame the area with 1-by-4-inch boards. Place a piece of masking tape on the back of each board and attach it to the wall flush to the floor. Frame doorways and openings by placing a brick or a block on the outer side, and then tape the board to the piece. Be sure the boards’ ends are flush together, creating a solid barrier around the room.
Mix the concrete according to the manufacturer's directions in a large bucket.
Begin spreading the concrete with a shovel. Pour the concrete slowly into the space and push it to the edge with a shovel. Initially smooth the concrete with the shovel’s backside. Work slowly and steadily, so you don’t apply severe pressure to the framing boards.
Smooth the concrete with a trowel. Even the concrete with a large trowel.
Remove the framing. Once the concrete is dry, cover the small opening between the new floor and the wall with baseboards.